Abstract
By isolating from the environment and precisely controlling mesoscopic objects, levitation in vacuum has evolved into a versatile technique that has already benefited diverse scientific directions, from force sensing and thermodynamics to materials science and chemistry. It also holds great promise for advancing the study of quantum mechanics in the unexplored macroscopic regime. However, most current levitation platforms are complex and bulky. Recent efforts in miniaturization of vacuum levitation set-ups have comprised electrostatic and optical traps, but robustness is still a concern for integration into confined settings, such as cryostats or portable devices. Here we show levitation and motion control in high vacuum of a silica nanoparticle at the surface of a hybrid optical–electrostatic chip. By combining fibre-based optical trapping and sensitive position detection with cold damping through planar electrodes, we cool the particle motion to a few hundred phonons. We envisage that our fully integrated platform is the starting point for on-chip devices combining integrated photonics and nanophotonics with precisely engineered electric potentials, enhancing control over the particle motion towards complex state preparation and read-out.
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Main
Since the seminal experiment by Ashkin et al., who reported the levitation in vacuum of a microsphere1, much progress has been made in controlling the translational and rotational degrees of freedom of levitated objects2. Although most efforts have focused on purely optical approaches, more recent developments have evolved towards hybrid platforms combining techniques adapted from atomic physics. For instance, to overcome the constraints posed by intense optical fields in terms of both photodamage and recoil heating3, researchers have introduced hybrid optical/electric potentials which combine spatial confinement with high potential depth4,5,6. Furthermore, linear feedback using electric forces on a charged particle7,8 enables more efficient cooling compared with its parametric counterpart9. Leveraging the palette of available techniques developed over the last decade has enabled the achievement of important milestones, including precision acceleration10,11 force12,13,14,15,16 and torque17 sensing, and achieving ground-state cooling in both one18,19,20,21,22 and two dimensions23.
As it gains maturity, vacuum levitation is now entering a phase of miniaturization, following the footsteps of trapped ions24 and solid-state25 systems. Beyond reducing bulkiness and mitigating instabilities associated with multiple assembled parts, on-chip integration is envisioned to facilitate advancements essential for the next generations of experiments. Nanoscale engineering at the chip surface can provide fine control over the electric26,27,28 and magnetic29 fields experienced by the particle. It also offers the possibility to enhance the nanoparticle’s interaction with optical fields by exploiting subwavelength modes supported by near-field nanocavities30. Interfacing with integrated photonics and meta-optics also has the potential to facilitate scalability towards arrays of multiple traps31,32,33. Finally, on-chip integration provides a pathway towards implementing on a single platform complex dynamic protocols involving bright and dark potentials34. Although miniaturization is well underway, with examples such as levitation in planar ion traps28,35,36 and optical trapping at the focus of a meta-lens37, fully integrated platforms are missing.
Here we present a hybrid photonic–electric on-chip platform enabling the robust levitation, precise position detection and dynamic control of a nanoparticle in vacuum. Our approach circumvents the need for bulky high-numerical-aperture (NA) lenses by combining commercial optical fibres with microscale additive manufacturing to create a robust, versatile and flexible optical interface. Despite the absence of focusing optics, we achieve high signal-to-noise ratios (SNRs) in optical displacement detection that compete with bulky, high-NA optics. When combined with active feedback cooling with planar electrodes, we efficiently cool down the particle motion in three dimensions.
Integrated hybrid optical–electric chip
Our levitation chip is structured in two layers: an upper photonic layer, where the particle is trapped, allowing precise detection of the nanoparticle’s motion through analysis of the scattered light; and a lower electric layer formed by a set of planar electrodes to cool the particle’s motion. To facilitate direct fibre interfacing, the photonic layer consists of an arrangement of four orthogonal cleaved single-mode optical fibres as illustrated in Fig. 1a. Trapping of the particle occurs in the standing-wave pattern formed by two interfering counterpropagating beams38,39. This configuration has the combined advantage of efficiently cancelling the scattering force while creating multiple trapping sites.
Let us first consider one single standing wave (SW) along y formed by two equally linearly polarized counterpropagating divergent beams as emerging from two single-mode fibres of NA = 0.1 (refs. 40,41), separated by a distance of d = 160 μm. The wavelength is λy = 1,550 nm and the total power P = 1 W. The equally linearly polarized light field interacts with a nanoparticle of refractive index nr, radius R = 160 nm and polarizability \(\alpha =4\uppi {\epsilon }_{0}{R}^{3}({n}_{\mathrm{r}}^{2}-1)/({n}_{\mathrm{r}}^{2}+2)\). At each intensity antinode, the optical force experienced by the particle gives rise to a harmonic potential with theoretical mechanical eigenfrequencies Ωx,y,z/(2π) ≈ (3.5, 89, 3.5) kHz and a trap depth U = 42kBT0, where kB is the Boltzmann constant and T0 = 300 K (room temperature). To achieve three-dimensional active feedback stabilization, it is necessary to ensure well-separated mechanical frequencies along each axis32. To this aim, we add a second SW with a wavelength λx = 1,064 nm along the x axis, as shown in Fig. 1a. The combination of both SWs results in a high-frequency mechanical mode along each optical axis (x and y) and a low-frequency mechanical mode (z) along the vertical axis.
Beyond ensuring robust trapping above the chip surface and an accurate adjustment of mechanical frequencies, the two pairs of optical fibres serve the additional purpose of monitoring the particle’s position by detecting its scattering. Exploiting the access to both optical axes, the scattered light from each SW is collected by the orthogonal fibre pair (arrows in Fig. 1a) and used to monitor the centre-of-mass (COM) motion. This distinctive collection scheme is inaccessible in single-beam traps and has the advantage of better adjusting to the scattering pattern of the particle42.
The fabricated chip measures 0.5 inches × 0.5 inches and is mounted on a custom-made printed circuit board (PCB) for electrical interfacing (Fig. 1b). The electrostatic layer consists of five planar electrodes (Fig. 1a,c), which are used to apply active electrical feedback via electric fields. To achieve reliable levitation, precise control over the position of each cleaved optical fibre is of upmost importance. Consequently, each individual fibre is held in two U-shaped mechanical mounts as shown in Fig. 1c. The latter are microfabricated via two-photon polymerization with a commercial Nanoscribe device (see Chip fabrication and printing of fibre mounts for further details). The relative fibre alignment is assessed by measuring the transmission T from fibre to fibre (Thorlabs SMF-28), as shown for 1,550 nm light for different fibre separations d in Fig. 2a. By fitting the data (circles) to a theoretical model (Supplementary Information, section I) we extract a relative fibre misalignment of δx ≈ 2.71 μm (dotted line). The dashed line shows the ideal case of no misalignment. Once aligned, the cleaved fibres are fixed with epoxy. During the curing process, the transmission T varies by a few percent, without significant long-term drifts at constant pressure (Supplementary Information, section I). Nevertheless, T consistently increases by around 4% from ambient pressure to vacuum. In general, T is stable over time, making this a reliable and robust method to position fibres permanently. Note that our fibre mounting method can be easily employed to create more complex optical lattices due to the arbitrary in-plane positioning of the fibres.
To maximize the trap depth, it is beneficial to position the fibre facets as close as possible to each other. Along y, this is limited by the diameter of the fibre cladding (125 μm, Thorlabs 1060XP). Along x, dx is limited by the diameter of the diverging 1,550 nm beam. To have a safety margin on these constraints and to diminish the interference coming from reflections, we work with dy = 160 μm and dx = 80 μm. The vertical distance between the nanoparticle and the chip surface is set to 203 μm. No additional fibre treatment or optics are employed for optical trapping.
Lens-free motional control on chip
Following standard nebulization-based loading, a single silica particle of radius R ≈ 160 nm is trapped at the intersection of the two SWs of wavelengths λx = 1,064 nm and λy = 1,550 nm. One distinctive feature of the intersecting SWs lies in the ability to independently tune the mechanical eigenfrequencies Ωq with q = x, y, z. As shown in Fig. 2b, by decreasing the power Px of the 1,064 nm SW, we observe the expected decrease of Ωx, while Ωy remains constant (dashed line). Additionally, by independently varying Px and Py of each SW and extracting Ωx (purple circles) and Ωy (blue triangles), we verify in Fig. 2c the expected behaviour as \({{{\Omega }}}_{\rm{q}}\propto \sqrt{{P}_{\rm{q}}}\) (dashed and dotted lines). Remarkably, despite the use of low-NA fibres, the achieved values of Ωq are comparable to those produced with high-NA optics.
The particle’s position along x, y is controlled by changing the relative phase ϕq between the corresponding counterpropagating beams (Supplementary Information, section II). In Fig. 2d, we move the particle along one axis and measure how much light is scattered into the fibre along the perpendicular direction. The blue triangles (purple circles) show the 1,064 nm (1,550 nm) power Px (Py) collected by the fibres along the y (x) axis. We attribute the shape of the 1,064 nm curve to the multimode character of the Thorlabs SMF-28 fibre at λx. To ensure high photon collection efficiency in both directions while maintaining symmetry, we place the particle in the position corresponding to x, y = 0.
To achieve high feedback efficiency, it is important to consider the angular distribution of the motional information radiation pattern42,43. For particles trapped by a single beam, most of the information about the particle’s axial motion is contained in the back-scattered light, enabling one-dimensional ground-state cooling via measurement-based feedback18,19,22. In contrast to the single-beam configuration, here the second trapping beam of the SW acts as a strong local oscillator with a fixed phase relation with respect to the back-scattered light. Efficient detection would then require separating the two light fields and using a local oscillator with the appropriate phase.
Instead, the information for the other degrees of freedom (DOF), especially the DOF perpendicular to the polarization axis, is scattered mainly perpendicularly to the beam propagation42. In our case, considering a SW along y polarized along z, the information about the x motion is scattered mainly the fibres along x (Supplementary Information, section III). This also applies to the y motion using the fibre along y. Hence, to detect the in-plane motion, we collect the scattered light at λy = 1,550 nm (λx = 1,064 nm) with the fibres along x (y) and use it in a balanced homodyne scheme to detect the motion along x (y). To detect the motion along the z direction, we use the second fibre along y. Here the multimode features of the SMF-28 fibre at λx = 1,064 nm allow the excitation of higher-order modes, increasing the sensitivity to displacements along z.
The power spectral densities (PSDs) of the motion along x, y, z at a pressure p = 14 mbar are plotted in Fig. 3 (dark blue). We reach an optimal SNRy ≈ 106, comparable to forward-scattering detection with high-NA optics in standard experiments44.
To cool and stabilize the nanoparticle’s COM motion in vacuum, we apply electrical cold damping7,8 along q = x, y, z. The nanoparticle’s COM motion is modelled as three decoupled harmonic oscillators described by the equation of motion
where m is the oscillator’s mass, Γm is the mechanical damping rate due to the surrounding gas, leading to a stochastic force \({F}_{\mathrm{th}}(t)=\)\(\sigma \eta (t)=\sqrt{2{k}_{\mathrm{B}}Tm{{{\varGamma }}}_{\mathrm{m}}}\eta (t)\) with ��(t) being white noise with unit standard deviation and zero mean45. The feedback force is proportional to the delayed position, that is, \({F}_{\rm{q}}^{{{\,{\rm{fb}}}}}(t)\propto {k}_{\rm{q}}^{\rm,d}\hspace{2.22144pt}q(t-\tau )\) where \({k}_{\rm{q}}^{\rm,d}\) is an adjustable gain and τ is a tunable delay. For τ = π/(2Ωq) this leads to an effective damping rate \({{{\varGamma }}}_{\rm{q}}^{{{{\rm{eff}}}}}={{{\varGamma }}}_{\mathrm{m}}+{{{\varGamma }}}_{\rm{q}}^{{{{\mathrm{fb}}}}}\) optimized for cooling7.
The externally applied feedback force \({F}_{\rm{q}}^{{{\,{\rm{fb}}}}}(t)=Q{E}_{\rm{q}}(t)\) depends on the charge of the particle Q = nqe− with nq elementary charges and the homogeneous electric field Eq(t) ∝ ±Vq(t) generated by planar electrodes as shown in Fig. 1a. For the in-plane DOF x(y), we apply two voltage signals ±Vx(t) (±Vy(t)) of equal amplitude but out of phase to the pair of electrodes situated left and right (top and bottom) of the chip. For cooling the z direction, we apply Vz(t) to a single planar electrode depicted in the centre of Fig. 1a. The symmetric electrode layout and the electrode–particle distance ensure the homogeneity of Eq(t) (Supplementary Information, section II).
The results of 3D cold damping on chip under a vacuum are shown in Fig. 3. The individual panels display the Lorentzian PSDs of the particle displacement \({S}_{\rm{q}}^{{{{\rm{IL}}}}}(\omega )\) at pressures p = 14 mbar (dark blue) and p = 9 × 10−6 mbar (light blue). In the latter, we stabilize the particle using active feedback in 3D.
Cooling and sensing performance
The lowest temperature \({T}_{\rm{q}}^{{{\,{\rm{eff}}}}}\) achievable in cold damping is determined by the detection noise σq and the mechanical damping Γm ∝ p (ref. 46). We fit the PSD of the in-loop (IL) detector7
to our data (Supplementary Information, section V). This allows us to determine the oscillator’s effective COM temperature \({T}_{\rm{q}}^{{{\,{\rm{eff}}}}}\) as
where \({{{\varGamma }}}_{\rm{q}}^{{{{\rm{fb}}}}}\propto \,{k}_{\rm{q}}^{\rm,d}\). The phonon occupation then is
Figure 4a displays the estimated phonon occupation 〈nq〉 for increasing feedback gain \({k}\,_{\rm{q}}^{\rm{d}}\) along the x (blue triangle) and y (purple circles) directions. The phonon occupation decreases to 〈ny〉 = 329 ± 30 and 〈nx〉 = 1,325 ± 72, respectively. The solid lines represent fits to equation (4) with the shaded regions indicating the uncertainty associated with the fitted curve (Supplementary Information, section VI). For large feedback gains, 〈nq〉 increases due to correlations between the detector noise σq and feedback signal, as depicted in Fig. 4a. In the PSD, it manifests as so-called noise squashing7,8,47, such that \({S}_{\rm{q}}^{{{{\rm{IL}}}}}({{{\varOmega }}}_{\rm{q}})\) yields underestimated values below the noise floor. This is depicted in Fig. 4b, where we plot the measured PSD of the y motion for different feedback gain values. Note that we use the in-loop detection signal for the temperature estimation. This approach remains valid, given that we account for the noise squashing by adding the second term in equation (3)7, making an out-of-loop detector unnecessary for the temperature estimation.
Due to its compact design and excellent cooling performance, the developed platform shows promise for application in force and acceleration sensing. The minimum force and acceleration sensitivity taking into account detection noise (Supplementary Information, section VII) exceeds the thermal limit and is given by
and is independent of the cooling of the COM. Yet, for real-life applications, the detection noise σq limits the bandwidth in which minimal sensitivities are achievable.
In Fig. 4c, we display the force and acceleration spectral densities, \(\sqrt{{S}_{\rm{y}}^{\mathrm{F}}}\) and \(\sqrt{{S}_{\rm{y}}^{\mathrm{a}}}\), for a range of \({k}_{\rm{y}}^{\rm,d}=[25,50,120]\). The solid line corresponds to equations (5) and (6) using the parameters extracted from the fitted in-loop PSDs. The experimentally achieved minimum sensitivities are \(\sqrt{{S}_{\rm{y}}^{\mathrm{F}}}=176\pm 26\,{\mathrm{zN}}\,{\mathrm{Hz}}^{-1/2}\) and \(\sqrt{{S}_{\rm{y}}^{\rm{a}}}=440\pm 70\,\upmu {\mathrm{g}}\,{\mathrm{Hz}}^{-1/2}\) which increase by 3 dB over an 8 kHz bandwidth around Ωy/(2π) = 59 kHz due to detector noise contributions exceeding the thermal noise. As expected, both bandwidth and sensitivities show no dependence of \({k}_{\rm{y}}^{\rm,d}\). Note that the hypothetical additional use of an out-of-loop detector would further deteriorate the sensitivities because we would have noise contributions from both detectors (Supplementary Information, section VII).
Conclusions
We have demonstrated robust optical on-chip levitation and motion control in vacuum with a fully integrated platform. Despite the use of commercial fibres with low NAs, we have shown that the particle’s displacement detection reaches comparable SNRs as with bulky high-NA optics. Such performance, which already enables the cooling of the COM down to hundreds of phonons, can be enhanced even more by further reducing the fibre distance.
The implemented platform also offers interesting applications towards multiparticle arrays32 beyond ten particles, optical binding31,48 and the levitation of high-refractive-index meta-atoms49. Additionally, as previously mentioned, our fabrication technique also enables more complex lattice forms50 by controlled in-plane fibre positioning.
Furthermore, the microfabricated fibre mounts are well suited for integrating a more controlled particle-loading mechanism51,52. By replacing one of the single-mode fibres with a hollow core fibre, individual particles could be delivered to the trapping region using an optical conveyor belt. To date this appears to be the only technique that offers deterministic particle loading into optical traps in ultrahigh-vacuum conditions53—an important prerequisite for the generation of macroscopic quantum states34,54.
In future versions of the platform, the integration of refractive microlenses55 or metalenses56,57 at the output facet of the fibres promises to enhance both detection sensitivity and achievable mechanical frequencies along the z axis. Furthermore, more complex optical elements such as fibre cavities58,59 can also be integrated. We envision our platform as the initial stepping stone towards the use of hybrid potentials for quantum experiments based on levitated particles.
Methods
Chip fabrication and printing of fibre mounts
The layer structure of our chip and the fabrication steps are illustrated in Extended Data Fig. 1. We start with a 530-μm-thick silicon 4 inch wafer with a 500-nm-thick silicon dioxide (SiO2) layer. The 500 nm oxide layer serves as an insulator layer to prevent electrical breakdown between the electrodes and the bulk silicon for voltages up to 235 V. Next, we evaporate a 5-nm-thick adhesion layer of titanium and a 100-nm-thick layer of gold.
To create the electrode pattern, the wafer is first spin coated with photoresist (AZ1512, 40 s at 4,000 rpm), baked for 60 s at T = 110 °C and exposed to a first mask using ultraviolet light. The resist is then developed and baked at T = 135 °C for 3 min. Then the gold is etched (TFA, Transene) for around 30 s, and subsequently the titanium is etched in hot hydrochloric acid (T = 90 °C) for around 60 s. The resist is then stripped off using acetone.
The next step is to etch the silicon oxide layer to create the clearance for printing the fibre mounts directly on silicon. We first spin coat the wafer with photoresist (AZ4562, 40 s at 1,500 rpm, resulting in a thickness of around 10 μm) and then bake it for 5 min at T = 110 °C. This is followed by a second round of mask exposure using ultraviolet light and development of the resist. The oxide is then etched using reactive-ion etching with fluoroform (CHF3) and argon for 33 min at 75 W. The resist is then stripped off using dimethylsulfoxide at 90 °C. Once the electrodes are patterned and the silicon oxide is etched, the wafer is diced into 0.5 inch × 0.5 inch samples.
The fibre mounts, shown in Fig. 1c, are then printed on each sample individually via dip-in two-photon lithography with a femtosecond laser lithography system (Photonic Professional GT, Nanoscribe). To increase the adhesion of the exposed IP-S resist (Nanoscribe) to the silicon subtrate we activate the surface using oxygen plasma (200 W for 30 s) and silanize it by immersing the chip into a mixture of 30 ml ethanol, 150 μl 3-(trimethoxysilyl)propyl methacrylate and 1.5 ml of acetic acid (1:10 acetic acid:water) for 30 min prior to the two-photon lithography. For printing, we use IP-S resist in combination with a 25× objective lens, which provides a printing area 400 μm in diameter. After the resist is exposed, the sample is developed in propylene glycol methyl ether acetate for 20 min and then rinsed with isopropyl alcohol for 3 min. Finally, the sample is glued to a PCB and the electrodes are connected to the board via wirebonding.
Data availability
Source data for Figs. 2, 3 and 4 are available via the ETH Zürich Research Collection at https://doi.org/10.3929/ethz-b-000667724.
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Acknowledgements
The authors acknowledge financial support from the European Commission through grant IQLev (grant agreement number 863132) and the European Research Council through grant Q-Xtreme ERC 2020-SyG (grant agreement number 951234).
Funding
Open access funding provided by Swiss Federal Institute of Technology Zurich.
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Contributions
B.M. and M.T.C. performed the measurements and analysed the data. G.F.M.T. and B.M. fabricated the device based on the design by M.T.C. and B.M. M.T.C. and N.M. developed the theoretical expressions. N.M. and R.Q. conceptualized the experiments. All the authors discussed the results and contributed to writing the manuscript.
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Nature Nanotechnology thanks Tania Monteiro and the other, anonymous, reviewer(s) for their contribution to the peer review of this work.
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Extended data
Extended Data Fig. 1 Fabrication of the on-chip platform.
a) The substrate is made of silicon covered with a layer of silicon oxide to isolate the substrate from the electrodes. The electrodes are made of gold, and a titanium layer is used to increase the adhesion of the electrodes to the silicon oxide. The fibre mounts are fabricated directly onto the silicon. b) Summarized fabrication process: 1. We start from a silicon wafer with a layer of silicon oxide. 2. The titanium and the gold are evaporated on the wafer. 3. The gold and the titanium are etched to create the electrodes. 4. The silicon oxide is etched to created the clearance for the fibre mounts. 5. After dicing the wafer, the fibre mounts are printed onto the silicon via two-photon polymerization. c) Fibre mounts used to align the fibres in our chip. The width of the square slot accommodating the fibre is chosen to be slightly smaller than the cladding of the single mode fibres.
Supplementary information
Supplementary Information
Supplementary sections I–VII and Figs. 1–7.
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Melo, B., T. Cuairan, M., Tomassi, G.F.M. et al. Vacuum levitation and motion control on chip. Nat. Nanotechnol. (2024). https://doi.org/10.1038/s41565-024-01677-3
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DOI: https://doi.org/10.1038/s41565-024-01677-3